Table 1 Data collection and refinement statistics.
From: Lipidic cubic phase injector facilitates membrane protein serial femtosecond crystallography
SMO/cyclopamine | |
|---|---|
Data collection | |
Space group | P21 |
Cell dimensions, | |
a, b, c (Å) | 40.5, 157.3, 52.4 |
α β γ (°) | 90.0, 97.0, 90.0 |
Resolution (Å) | 40–3.20 (3.26–3.20)* |
Rsplit, (%) | 9.8 (63.2) |
I/σ(I) | 7.4 (1.8) |
CC* | 0.9991 (0.28) |
Completeness (%) | 100 (100) |
Multiplicity | 2,515 (1,820) |
Refinement | |
Resolution (Å) | 40–3.20 |
Anisotropic truncation (Å) | 3.4, 3.2, 4.0 |
No. reflections/test set | 8,082/399 |
Rwork/Rfree | 0.232/0.278 |
No. atoms | |
Protein | 3,389 |
Cyclopamine | 30 |
B -factors (Å2) | |
Wilson B/overall B | 101.6/78.4 |
Receptor/BRIL | 76.8/83.7 |
Cyclopamine | 76.3 |
R.m.s. deviations | |
Bonds lengths(Å) | 0.003 |
Bond angles (°) | 0.61 |
