Fig. 3: Gram-scale preparation and synthetic applications.
From: Practical and regioselective halonitrooxylation of olefins to access β-halonitrates
a Scale-up reaction of chloro-, bromo-, and iodo-nitrooxylation. b Synthetic applications of 106. c Synthetic applications of 47. aScale-up reaction was carried out based on Condition A depicted in Fig. 2. bScale-up reaction was carried out based on Condition B depicted in Fig. 2. THF tetrahydrofuran, DMSO dimethyl sulfoxide, rt room temperature, DMF N,N-dimethylformamide, Cbz benzyloxycarbonyl.
