Fig. 2: Structure characterisation and analysis of mCOF-Ag.
From: Single crystal of a one-dimensional metallo-covalent organic framework
a 3D reciprocal lattice of mCOF-Ag reconstructed from the SCED data (left) and 2D slices cut from the reconstructed reciprocal lattice (right). b SEM image of mCOF-Ag with uniform rod-like morphology. Scale bar: 1 µm. c HRTEM image of mCOF-Ag and SAED pattern (inset) confirmed the single-crystal nature of the material. Scale bar: 20 nm. d Observed electron density map of the initial structure model determined from SCED data along the c-axis.
