Table 1 Hydrodynamic diameter \(\langle D_h\rangle\), particle diameter \(\langle D_P\rangle\), core diameter \(\langle D_C\rangle\) and diameter of the core fragments \(\langle D_F\rangle\) as determined by DLS, low-magnification HAADF-STEM, HRTEM and XRD.
| Â | \(\langle D_h\rangle\,[\text{nm}]\) | \(\langle D_P\rangle\,[\text{nm}]\) | \(\langle D_C\rangle\,[\text{nm}]\) | \(\langle D_F\rangle\,[\text{nm}]\) |
|---|---|---|---|---|
DLS | \(29\pm 8\) | – | – | – |
HAADF-STEM | – | \(20\pm 4\) | \(15\pm 4\) | – |
HRTEM | – | \(19\pm 4\) | \(13\pm 3\) | \(9\pm 3\) |
XRD | – | \(16\pm 3\) | \(7\pm 1\) | |
